sodium methoxide oor Spaans
sodium methoxide
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Sodium methoxide is used as the base because the reactants are methyl esters.
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The secondary alcohol is mixed directly with DCC, formic acid, and a strong base such as sodium methoxide.
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Sodium methoxide is highly caustic and reacts with water to give methanol, which is toxic and volatile.
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m-Fluoronitrobenzene reacts with sodium methoxide 105 times more slowly than its ortho and para isomers.
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Like sodium acetylide, sodium methoxide (NaOCH3) is an ionic compound.
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Vinylic halides, such as PhCH=CHBr, are converted to the unsaturated esters upon treatment with Ni(CO)4 followed by sodium methoxide.
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Sodium methoxide is prepared by carefully treating methanol with sodium: 2 Na + 2 CH 3OH → 2 CH 3ONa + H 2 The reaction is so exothermic that ignition is possible.
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The resulting solution, which is colorless, is often used as a source of sodium methoxide, but the pure material can be isolated by evaporation followed by heating to remove residual methanol.
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The derivatization of triglycerides and fatty acids had methylation reaction with sodium methoxide for 45 minutes, and for 15 minutes with boron trifluoride, ending with the quantification of methyl esters of fatty acids by gas chromatography.
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The reactions were carried out in a polar aprotic solvent such as N, N-dimethylformamide (DMF) or dimethylsulfoxide (DMSO), in the presence of a base such as sodium hydride or sodium methoxide in anhydrous conditions, from 50 °C to 100 °C.
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Methods: The evaluated conditions were the quantity and type of organic solvents (sodium methoxide 250 μL and 500 μL; boron triflouride 700 μL), quantity of sample (3.0 g and 6.0 g) and fat extraction method used according to Folch et al., 1957 (9).
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Conclusions: Quantification of fatty acid methyl esters in beef by gas chromatography was shown to be effective and there was no statistical difference when comparing the amount of meat sample, type of reagent (sodium methoxide or boron trifluoride) and reagent volume employed in the derivatization step.
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Objectives: Determination of the best conditions for the quantification of methyl esters, varying some conditions like the amount of meat and the volume of sodium methoxide or boron trifluoride used in the derivatization step of an analytical method used for determination of lipid profile in beef meat.
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Sodium methoxide - Wikipedia, the free encyclopedia
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The structure, and hence its basicity, of sodium methoxide in solution depends on the solvent.
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In the solid form, sodium methoxide is polymeric, with a sheet-like arrays of Na+ centers, each bonded to four oxygen centers.
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The diagrams below show typical results of the transesterification of rapeseed oil (industrial grade) with sodium methoxide (left) and potassium hydroxide (right).
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The 5-methoxytriazole precursor to this carbene was made by the treatment of a triazolium salt with sodium methoxide, which attacks as a nucleophile.
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In a glass put some sunflower oil, other prepared the reagent: methanol with dissolved caustic soda, which is called sodium methoxide (this must be handled with care, is flammable, toxic and corrosive).
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With the lid off, turn your blender on its slowest setting, and begin slowly adding the lye to the methanol inside. This will create sodium methoxide, but take precaution that the mixture doesn't splatter all over.
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Dichloroacetic acid method of sodium methoxide and methanol into the reaction tank, heated to 40 ~ 50 °C, slowly dropping dichloroacetic acid, after the completion of reflux reaction 2h, condensation is completed, and then cooled to room temperature, filtration, methanol washing, Combined to wash the filtrate, that was dimethoxy acetic acid sodium methanol solution.
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